IMPROVING THE MECHANICAL PROPERTIES OF GLASS IONOMER CEMENT
Abstract
Background: Glass ionomer cement (GIC) exhibits limitations such as low mechanical strength, poor fracture resistance, and limited durability, restricting its clinical applications. This study aimed to evaluate the impact of nano-hydroxyapatite( nHA) incorporation on the mechanical properties of GIC, focusing on tensile strength, fracture resistance, fatigue limit, and microhardness.
Materials & Methods: Study type is experimental , the research is done in faculty of dentistry, University of Almaarif, Alanbar, Iraq. All samples were collected and tested in a duration of two year (2023 to 2025). A total of 50 GIC formulations were prepared, divided into control (25 samples without nHA) and modified (25 samples with nHA) groups. Mechanical tests were performed to measure tensile strength, fracture resistance, fatigue limit, and microhardness. Data were analyzed statistically to compare the two groups .
Results: The modified GIC group exhibited significantly higher tensile strength (25.41 MPa vs. 20.21 MPa), fracture resistance (101.48 N vs. 84.15 N), fatigue limit (12,659 cycles vs. 8,095 cycles), and microhardness (62.80 VHN vs. 48.27 VHN) compared to the control group (p < 0.05 for all). Regression analysis highlighted tensile strength and fracture resistance as strong predictors of microhardness.
Conclusion: The incorporation of nHA significantly improved the mechanical properties of GIC, making it a promising material for dental restorations requiring enhanced strength and durability.
Keywords
Full Text:
PDFReferences
Murugan R, Yazid F, Nasruddin NS, Anuar NNM. Effects of nanohydroxyapatite incorporation into glass ionomer cement (GIC). Minerals. 2021;12(1):9. https://doi.org/10.3390/min12010009
Makanjuola J, Deb S. Chemically activated glass-ionomer cements as bioactive materials in dentistry: a review. Prosthesis. 2023;5(1):327–45. https://doi.org/10.3390/prosthesis5010024
Nicholson JW, Sidhu SK, Czarnecka B. Enhancing the mechanical properties of glass-ionomer dental cements: a review. Materials. 2020;13(11):2510. https://doi.org/10.3390/ma13112510
Yang Z, Han L, Guo Y, Jia L, Yin C, Xia Y. Nanotechnology in dental therapy and oral tissue regeneration. Nanotechnology in Regenerative Medicine and Drug Delivery Therapy. 2020:91–189. https://doi.org/10.1007/978-981-15-5386-8_3
Saran R, Upadhya NP, Ginjupalli K, Amalan A, Rao B, Kumar S. Effect on physical and mechanical properties of conventional glass ionomer luting cements by incorporation of all-ceramic additives: an in vitro study. Int J Dent. 2020;2020:8896225. https://doi.org/10.1155/2020/8896225
Kang S, Park SJ, Kim S, Kang I-K. Chemical bonding of nanorod hydroxyapatite to the surface of calciumfluoroaluminosilicate particles for improving the histocompatibility of glass ionomer cement. Coatings. 2024;14(7):893. https://doi.org/10.3390/coatings14070893
Shirazi M, Pirzeh A, Atashgaran M. Antimicrobial properties of glass-ionomer cement incorporated with nano-hydroxyapatite against mutans streptococci and lactobacilli under orthodontic bands: an in vivo split-mouth study. Dent Res J. 2024;21(1):1. https://doi.org/10.4103/drj.drj_240_23
Daokar SG, Patel KK, Pawar KS, Wahane KD, Kulkarni SS, Mantri AR. Evaluation of bonding strength of conventional glass ionomer cement modified with micro- and nano-hydroxyapatite: an in vitro study. J Interdiscip Dent. 2021;11(3):114–8. https://doi.org/10.4103/jid.jid_76_20
Ramić B, Cvjetićanin M, Bajkin B, Drobac M, Milanović M, Rajnović D, et al. Physical and mechanical properties assessment of glass ionomer cements modified with TiO2 and Mg-doped hydroxyapatite nanoparticles. J Appl Biomater Funct Mater. 2024;22:22808000241282184. https://doi.org/10.1177/22808000241282184
Pérez-Castro B, Flores-Ledesma A, Rubio-Rosas E, Teutle-Coyotecatl B, Flores-Ferreyra BI, Argueta-Figueroa L, et al. Comparison of the physical properties of glass ionomer modified with silver phosphate/hydroxyapatite or titanium dioxide nanoparticles: in vitro study. J Clin Pediatr Dent. 2024;48(4):160–7. https://doi.org/10.22514/jocpd.2024.089
Ilancheran P, Paulraj J, Maiti S, Shanmugam R. Green synthesis, characterization, and evaluation of the antimicrobial properties and compressive strength of hydroxyapatite nanoparticle-incorporated glass ionomer cement. Cureus. 2024;16(4):e58562. https://doi.org/10.7759/cureus.58562
Ivanišević A, Rajić VB, Pilipović A, Par M, Ivanković H, Baraba A. Compressive strength of conventional glass ionomer cement modified with TiO2 nano-powder and marine-derived HAp micro-powder. Materials. 2021;14(17):4964. https://doi.org/10.3390/ma14174964
Wan Jusoh WN, Matori KA, Mohd Zaid MH, Zainuddin N, Ahmad Khiri MZ, Abdul Rahman NA, et al. Incorporation of hydroxyapatite into glass ionomer cement (GIC) formulated based on alumino-silicate-fluoride glass ceramics from waste materials. Materials. 2021;14(4):954. https://doi.org/10.3390/ma14040954
Mederos M, Cuevas-Suarez CE, Sanchez W, Miranda P, Francia A, Pardo H, et al. Effect of the incorporation of hydroxyapatite on the diametral tensile strength of conventional and hybrid glass ionomer cements. Odontology. 2021;109(4):904–11. https://doi.org/10.1007/s10266-021-00624-1
Piyush G, Kalyan SS, Aparna UP, Khyati G, Basawaraj B. Effects of novel additives on the mechanical and biological properties of glass ionomer cement: an in vitro study. J Conserv Dent Endod. 2024;27(5):503–7. https://doi.org/10.4103/JCDE.JCDE_81_24
Ravi B, Paulraj J, Maiti S, Shanmugam R. Assessing the influence of thermocycling on compressive strength, flexural strength, and microhardness in green-mediated nanocomposite-enhanced glass ionomer cement compared to traditional glass ionomer cement. Cureus. 2024;16(3):e56078. https://doi.org/10.7759/cureus.56078
Caesarianto F, Nurlely, editors. The enhancement of glass ionomer cement mechanical strength through the incorporation of fluorhydroxyapatite nanocrystals. AIP Conf Proc. 2021. https://doi.org/10.1063/5.0047819
Sharafeddin F, Jowkar Z, Bahrani S. Comparison between the effect of adding microhydroxyapatite and chitosan on surface roughness and microhardness of resin modified and conventional glass ionomer cements. J Clin Exp Dent. 2021;13(8):e737. https://doi.org/10.4317/jced.55996
Abdulmunem M, Kutty MG, Abd Majid WH, Dabbagh A, Abu Kasim NH, Yahya NA, et al. The effect of bioactive glass and sintering conditions on the properties of titanium-hydroxyapatite composites. Sains Malaysiana. 2021;50(4):1089–99. https://doi.org/10.17576/jsm-2021-5004-19
Abdulmunem M, Dabbagh A, Abdullah HB, Hayaty N, Kasim A. The combined effect of dental post and cement materials on fracture resistance and fracture mode of endodontically treated teeth. Sains Malaysiana. 2015;44(8):1189–94. https://doi.org/10.17576/jsm-2015-4408-16
DOI: https://doi.org/10.46903/gjms/23.3.1958
Refbacks
- There are currently no refbacks.
Copyright (c) 2025. Mohamed Abdulmunem

This work is licensed under a Creative Commons Attribution-NonCommercial 4.0 International License.

Gomal Medical College, Daraban Road, Dera Ismail Khan, Pakistan
ISSN: 1819-7973, e-ISSN: 1997-2067
Website: https://www.gmcdikhan.edu.pk
Phone: +92-966-747373

